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ChemInform Abstract: Reductive Opening of Phenyl Substituted Thiacycloalkanes: New Way for Sulfur-Containing Organolithium Compounds.

✍ Scribed by J. ALMENA; F. FOUBELO; M. YUS

Book ID: 101842994
Publisher: John Wiley and Sons
Year: 2010
Weight: 31 KB
Volume: 28
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199730091

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The reaction of 2-phenyl substituted four, five and six membered thiacycloalkanes (1, 4 and 7) with lithium and a catalytic amount of DTBB (5 mol %) in THF at -78°C leads to the corresponding sulphur-containing benzylic organolithium compounds (2, 5 and 8), which by reaction with different electxoph

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