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ChemInform Abstract: Reaction of Cyclohexa-1,2,3-triene with N,α-Diphenylnitrone: Formation of Seven-Membered Cyclic Amines via Piradone Derivatives.

✍ Scribed by Michihito Sakura; Shinichi Ando; Atsushi Hattori; Katsuhiro Saito


Publisher
John Wiley and Sons
Year
2010
Weight
31 KB
Volume
30
Category
Article
ISSN
0931-7597

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✦ Synopsis


Reaction of Cyclohexa-1,2,3-triene with N,α-Diphenylnitrone: Formation of Seven-Membered Cyclic Amines via Piradone Derivatives.

-Treatment of the triflate (I) with CsF generates cyclohexa-1,2,3-triene, the smallest cyclic allene known to undergo fast dimerization. However, it can be trapped by diarylnitrones (II) to yield the benzazepinones (III). -