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ChemInform Abstract: Preparation of Sn-, Ge-, and Si-Heterocycles from Zirconacycles.

✍ Scribed by Yasuyuki Ura; Yanzhong Li; Fu-Yu Tsai; Kiyohiko Nakajima; Martin Kotora; Tamotsu Takahashi

Publisher: John Wiley and Sons
Year: 2010
Weight: 32 KB
Volume: 31
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200030160

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Preparation of the Compounds R3ElHgElR3

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imide as a colorless oil ([a]: = +57 O , c = 1.2 in chloroform) which yielded theester (4) (m.p.114-115 "C, [alg=-35f 3 ' . c = 0.9 in chloroform) on hydrolysis (3 hours' boiling with 5 N HCI) and subsequent esterification with p-bromophenacyl bromide. No depression of melting point was observed wit