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ChemInform Abstract: Preparation of Chiral Building Blocks for the Synthesis of Aconitium Alkaloids.

✍ Scribed by M. IHARA; M. SUZUKI; A. HIRABAYASHI; Y. TOKUNAGA; K. FUKUMOTO

Book ID
112024835
Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
27
Category
Article
ISSN
0931-7597

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Preparation of chiral building blocks fo
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Treatment of meso-diols 3 and 6 with CCL and vinyl acetate without solvent produced the AE part of Aconitium alkaloids 2 and 7 in 68% and 75% yields, respectively, with > 96% e.e. Quantitative formations of their MTPA esters 4 and 8 were achieved by reaction with MTPA in the presence of DCC and DMAP

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## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a β€œFull Text” option. The original article is trackable v

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For recent reviews and highlights on dendrimers, see [I]. ' ) The compound that would result from the reduction of 10 can, however, be prepared by a simpler procedure, see Scheme 2.