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ChemInform Abstract: Practical Entry into the HIJKLM Ring Segment of Ciguatoxin CTX3C.

✍ Scribed by Tohru Oishi; Hisatoshi Uehara; Yoko Nagumo; Mitsuru Shoji; Jean-Yves Le Brazidec; Masashi Kosaka; Masahiro Hirama

Publisher: John Wiley and Sons
Year: 2010
Weight: 31 KB
Volume: 32
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200123208

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A Facile Entry into the Ring System of Sativene. -Careful bromination of the diketone (I) allows the synthesis of the dibromides (II) and (III) or corresponding tribromide (IV). Their DBU-mediated dehydrobromination leads to tricyclic compounds of which (V) and (VII) have the same carbon skeleton a