The use of the PCl 3 /hydrazone/dicarboxylic acid combination can be applied in an efficient one-pot procedure for the synthesis at room temperature of the seven-membered ring compounds, 6 (perhydro-1,4,5-oxadiazepine-3,6-diones) and (perhydro-1,4,5-thiadiazepine-3,6-diones), and of the first report
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ChemInform Abstract: PCl3-Mediated Cyclization: Synthesis at Room Temperature of N-Alkenyl Derivatives of Perhydro-1,4,5-oxa(and thia)diazepine-3,6-dione and of 6,7-Diazaspiro[3.4]octane-5,8-dione.
β Scribed by Graziano Baccolini; Carla Boga; Umberto Negri
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 35 KB
- Volume
- 31
- Category
- Article
- ISSN
- 0931-7597
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