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ChemInform Abstract: Novel Stereoselective Synthesis of Glycosyl-1-O-acyl Esters via Peracetylglycosyl Phosphorothioates, -selenoates and -dithioates as Glycosyl Donors.

✍ Scribed by J. BOROWIECKA; M. MICHALSKA

Book ID: 112040832
Publisher: John Wiley and Sons
Year: 2010
Weight: 36 KB
Volume: 27
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199648234

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✍ J. BOROWIECKA 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 30 KB 👁 2 views

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Highly Stereoselective Synthesis of the 1-O-Acylglycosyl Ester of Diclofenac via Glycosyl Phosphorothioates, -Selenoates and -Dithioates as Glycosyl Donors

✍ Borowiecka, Joanna 📂 Article 📅 1997 🏛 John Wiley and Sons 🌐 English ⚖ 418 KB

## Abstract Stereoselective glycosylation of __o__‐(2,6‐dichloroanilino)phenylacetic acid (Diclofenac, 1), as a free carboxylic acid with glycosylthio (2a–c), ‐dithio (3a–e) and ‐selenophosphates (4a–c) as glycosyl donors is reported. The reactions were carried out in aprotic solvents, in the prese