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ChemInform Abstract: New Methodology for the Differentiation of the Primary Hydroxyl Groups in 2,3,3′,4,4′-Penta-O-benzylsucrose: Convenient Approach to Sucrose Monophosphines.

✍ Scribed by Joanna Burdynska; Bartosz Lewandowski; Slawomir Jarosz

Publisher: John Wiley and Sons
Year: 2011
Weight: 50 KB
Volume: 42
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.201140189

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✦ Synopsis

Abstract

The reaction of penta‐O‐benzyl sucrose (I) with tert‐butyldiphenylsilyl chloride proceeds regioselectively to afford 6′‐O‐silyl derivative (III), which is used for the synthesis of iodide (VI).

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