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ChemInform Abstract: Montmorillonite Clay Catalysis. Part 4. An Efficient and Convenient Procedure for Preparation of 1,1-Diacetates from Aldehydes.

✍ Scribed by Z.-H. ZHANG; T.-S. LI; C.-G. FU

Publisher
John Wiley and Sons
Year
2010
Weight
28 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

Montmorillonite Clay Catalysis. Part 4. An Efficient and Convenient

Procedure for Preparation of 1,1-Diacetates from Aldehydes.

-An alternative preparation of title compounds, e.g. (III) and (V), with the advantages of selectivity, operational simplicity, high yields, short reaction times, ease of work-up and minimal environmental impact, is provided. The scope and limitation of this method are also investigated. -(ZHANG, Z.-H.;

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An Efficient and Convenient Procedure for the Synthesis of 1,1-Diacetates of Aldehydes Catalyzed by Anhydrous Ferrous Sulfate. -A series of 1,1-diacetates (III) is readily synthesized from aldehydes (I) in excellent yields by reaction with acetic anhydride using anhydrous ferrous sulfate as catalys