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ChemInform Abstract: Microwave Assisted, Highly Efficient Solid State N- and S-Alkylation.

✍ Scribed by Harsha G. Jaisinghani; Bhushan M. Khadilkar

Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
30
Category
Article
ISSN
0931-7597

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✦ Synopsis

Microwave Assisted, Highly Efficient Solid State N-and S-Alkylation.

-Secondary amines and thiophenols are alkylated with alkyl or benzyl halides on alumina-supported potassium carbonate under solvent-free conditions using microwaves. The method does not require a strong base nor a phase-transfer catalyst. Reaction times of 2-23 minutes are necessary. In the case of the monoalkylation of aniline four equivalents of anilines are used. -(JAISING-

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