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ChemInform Abstract: Mercury(II) Diphosphate, Hg2P2O7.

✍ Scribed by M. WEIL; R. GLAUM

Publisher
John Wiley and Sons
Year
2010
Weight
28 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

1997 structure structure (solids and liquids) D 2000

46 -005

Mercury(II) Diphosphate, Hg2P2O7.

-Polycrystalline Hg2P2O7 is prepared by heating a solution of HgO in 50% HNO3 with a small excess of H3PO4 followed by annealing of the residue at 693 K in air (4 d, silica crucible). Single crystals are obtained via chemical vapor transport with PCl5 (823 β†’ 773 K, 19 d). Hg2P2O7 crystallizes in the triclinic system, space group P1, Z = 2. The compound is isotypic with Cd2P2O7. The structure consists of alternating layers of P2O7 groups and HgO6 polyhedra, respectively.

-(WEIL, M.;

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