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ChemInform Abstract: K3Au5Pb: Layers of 2∞[AuAu3/2] Gold Tetrahedra and 1∞[Pb2/2] Lead Chains.

✍ Scribed by U. ZACHWIEJA; J. WLODARSKI

Publisher
John Wiley and Sons
Year
2010
Weight
34 KB
Volume
29
Category
Article
ISSN
0931-7597

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✦ Synopsis

Lead Chains.

-Single crystals of K 3 Au 5 Pb are obtained by reaction of KN 3 with gold sponge and lead powder at 920 K. The compound crystallizes in a novel structure type, which can be described as a substitution variant of the MgCu 2 -type (space group Imma, Z = 4). The gold-lead partial structure consists of layers of 2 ∞[AuAu3/2] tetrahedra and 1 ∞[Pb2/2] zigzag chains with four-bonded lead atoms which are connected to a framework structure via Au-Pb contacts. The K atoms occupy channels within the gold lead partial structure. -(ZACHWIEJA, U.;

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