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ChemInform Abstract: Intramolecular Cyclization of ω-Haloalkyl-Substituted Thiophosphorylacetonitriles: Synthesis and Stereochemistry of 3-Cyano-2-oxo-1,2-thiaphosphacyclanes.

✍ Scribed by Irene L. Odinets; Natalya M. Vinogradova; Konstantin A. Lyssenko; Michail Yu. Antipin; Pavel V. Petrovskii; Tatyana A. Mastryukova

Publisher
John Wiley and Sons
Year
2010
Weight
39 KB
Volume
33
Category
Article
ISSN
0931-7597

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Intramolecular cyclization of ω-haloalky
Intramolecular cyclization of ω-haloalkylsubstituted thiophosphorylacetonitriles: Synthesis and stereochemistry of 3-cyano-2-oxo-1,2-thiaphosphacyclanes
✍ Irene L. Odinets; Natalya M. Vinogradova; Konstantin A. Lyssenko; Michail Yu. An 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 English ⚖ 295 KB

## Abstract Intramolecular S‐alkylation in a series of ω‐haloalkyl‐substituted thiophosphorylacetonitriles **__5–7__** presents an effective synthetic route to the hitherto unknown 3‐cyano‐2‐oxo‐1,2‐thiaphospholanes **__14__** and thiaphosphinanes **__15__**. The compounds were obtained as a mixtur