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ChemInform Abstract: Green, Catalyst-Free Thioacetalization of Carbonyl Compounds Using Glycerol as Recyclable Solvent.

✍ Scribed by Gelson Perin; Luzia G. Mello; Catia S. Radatz; Lucielli Savegnago; Diego Alves; Raquel G. Jacob; Eder J. Lenardao

Publisher
John Wiley and Sons
Year
2010
Weight
22 KB
Volume
41
Category
Article
ISSN
0931-7597

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Solvent-Free Thioacetalization of Carbonyl Compounds Catalyzed by Cu(OTf ) 2 -SiO 2 . -Copper(II) triflate on silica gel (activated at 120 β€’ C at 1mm Hg for 6h) allows the solvent-free thioacetalization of aldehydes and ketones in an efficient manner.