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ChemInform Abstract: Glycosylation of Silybin.

✍ Scribed by V. KREN; J. KUBISCH; P. SEDMERA; P. HALADA; V. PRIKRYLOVA; A. JEGOROV; L. CVAK; R. GEBHARDT; J. ULRICHOVA; V. SIMANEK

Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

Glycosylation of Silybin.

-In order to obtain more soluble derivatives of natural silybin (I), which is an equimolar mixture of two diastereomers, glycosides such as (III) and (IV) are synthesized under optimized conditions. It is noteworthy that the use of TmsOTf or SnCl4 as Lewis acids or the condition of Helferich gives lower yields.

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