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ChemInform Abstract: Fmoc-Peptide Acid Chlorides: Preparation, Characterization and Utility in Peptide Synthesis.

โœ Scribed by K. GAYATHRI; H. N. GOPI; V. V. S. BABU

Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
29
Category
Article
ISSN
0931-7597

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โœฆ Synopsis

Fmoc-Peptide Acid Chlorides: Preparation, Characterization and Utility in Peptide Synthesis.

-Acid chlorides, e.g. (II), are isolated as crystalline solids, which can be stored for long periods under anhydrous conditions. As exemplified by the preparation of peptide (IV) these acid chlorides can be used as coupling reagents in peptide synthesis. -(GAYATHRI, K.;

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## Abstract For Abstract see ChemInform Abstract in Full Text.

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Established methodology for the preparation of peptide thioesters requires the use of t-butoxycarbonyl chemistry owing to the lability of thioester linkers to the nucleophilic reagents used in Fmoc solid phase peptide synthesis. Both the greater ease of use and the broad applicability of the method