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ChemInform Abstract: Facile Synthesis of the Tridecameric Al13 Nanocluster Al13(μ3-OH)6 (μ2-OH)18(H2O)24 (NO3)15.

✍ Scribed by Jason T. Gatlin; Zachary L. Mensinger; Lev N. Zakharov; David MacInnes; Darren Johnson

Publisher
John Wiley and Sons
Year
2008
Weight
34 KB
Volume
39
Category
Article
ISSN
0931-7597

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ChemInform Abstract: Synthesis of the Hydroxide Cluster [Al13(μ3-OH)6(μ-OH)18 (H2O)24]15+ from an Aqueous Solution.
✍ Wei Wang; Katherine M. Wentz; Sophia E. Hayes; Darren W. Johnson; Douglas A. Kes 📂 Article 📅 2011 🏛 John Wiley and Sons ⚖ 20 KB 👁 1 views

Synthesis of the Hydroxide Cluster [Al 13 (μ 3 -OH) 6 (μ-OH) 18 (H 2 O) 24 ] 15+ from an Aqueous Solution. -[Al13(μ3-OH)6(μ-OH)18(H2O)24](NO3)15 is synthesized by treatment of an aqueous solution of Al(NO3)3 with Zn metal powder (Al:Zn = 2:1) at room temperature (55% yield). The single crystal XRD r