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ChemInform Abstract: Facile One-Pot Synthesis of [1,2,4]Triazolo[3,4-b][1,3,4]thiadiazines and 3,7-Dimethyl-4H-[1,2,4]triazino[3,4-b][1,3,4]thiadiazin-6-one Using Heteropolyacid Catalysis.

✍ Scribed by Radineh Motamedi; Aazam Monfared; Zohre Ghahghai Nezamabadi; Fatemeh F. Bamoharram

Publisher
John Wiley and Sons
Year
2011
Weight
30 KB
Volume
42
Category
Article
ISSN
0931-7597

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The reaction of 3-mercapto-4-aryIideneamino-l,2,4triazoles 2b-d, 3a-d with ethyl bromoacetate and/or phenacyl bromide in hot DMF and triethylamine affords the stereochemically pure 7-acyl-6-aryl-6,7dihydro-5H-lt2, 4-triazolo[3,4-b][l, 3,4]thiadiazines