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ChemInform Abstract: Electrolytic Partial Fluorination of Organic Compounds. Part 29. Anodic Mono- and Difluorination of 2-Benzoxazolyl Sulfides.

✍ Scribed by Kamal M. Dawood; Seiichiro Higashiya; Yankun Hou; Toshio Fuchigami

Publisher: John Wiley and Sons
Year: 2010
Weight: 32 KB
Volume: 30
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199922059

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✦ Synopsis

Electrolytic Partial Fluorination of Organic Compounds. Part 29. Anodic Mono-and Difluorination of 2-Benzoxazolyl Sulfides.

-Anodic fluorination of readily achieved 2-benzoxazolyl sulfides (III) by fluoride salts in DME as solvent provides mono-and difluorinated products in reasonable yields. Monofluorination at the α-position to the sulfur atom takes place preferentially. Expected products of α,α-difluorination are not observed, but products fluorinated at both the α-position and the benzene ring (presumably at the 5-or 6-position). Interestingly, so far not reported anodic fluorination of the electrolytic solvent DME is observed as a side reaction. -(DAWOOD,

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