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ChemInform Abstract: Crystal Structures of the Tellurates Pb3Fe2Te2O12 and Pb2CoTeO6.

✍ Scribed by B. WEDEL; HK. MUELLER-BUSCHBAUM

Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

1997 structure structure (solids and liquids) D 2000

19 -013

Crystal Structures of the Tellurates Pb3Fe2Te2O12 and Pb2CoTeO6.

-Single crystals of the title compounds are prepared by reaction of PbO and Fe2O3 or CoO in a TeO2 flux (corundum crucible, air, 730 β€’ C, 48 h). Pb3Fe2Te2O12 crystallizes in the monoclinic space group Cc with Z = 4. Its structure is characterized by a network of corner-and edge-sharing O6 octahedra centered by Fe3+ and Te6+ in a disordered manner. The structure exhibits large cavities which are occupied by the Pb2+ ions. Pb2CoTeO6 has the tetragonal elpasolithe type structure,

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