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ChemInform Abstract: Crystal Structure of a Quaternary Nd—Ni—Si—B Compound — Refinement of Synchrotron Radiation Data.

✍ Scribed by E. WU; H. ZHANG; S. J. CAMPBELL; S. R. BULCOCK

Publisher
John Wiley and Sons
Year
2010
Weight
36 KB
Volume
29
Category
Article
ISSN
0931-7597

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✦ Synopsis

1998 structure structure (solids and liquids) D 2000

18 -009

Crystal Structure of a Quaternary Nd-Ni-Si-B Compound -Refinement of Synchrotron Radiation Data.

-A sample of nominal composition NdNi 8 SiB 3 is synthesized by arc melting of the corresponding elements and subsequent annealing in a sealed evacuated quartz tube at 900 • C for two weeks. The crystal structure of this new phase is determined from a Rietveld profile refinement of synchrotron radiation data. The refined compound crystallizes in a tetragonal unit cell (space group P4/nmm) and corresponds to a main phase composition of ≈NdNi 9.7

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