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ChemInform Abstract: Convenient and Practical Synthesis of (R)-(+)-4-Methyl-2-cyclohexen-1- one.

✍ Scribed by H. W. LEE; S. K. JI; I.-Y. C. LEE; J. H. LEE

Book ID
112036033
Publisher
John Wiley and Sons
Year
2010
Weight
28 KB
Volume
27
Category
Article
ISSN
0931-7597

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## Abstract The title compound __R__‐4a was prepared from (–)‐quinic acid (1) in 6 steps in 18% overall yield (Scheme 3) and with 100% enantiomeric purity (Figure 1). The initiating step is the regio‐ and stereoselective acetalization of the __trans__‐oriented vicinal OH groups of 1 (+ 5 β†’ 8). Alco