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ChemInform Abstract: Convenient Access to Isoindolinones via Carbamoyl Radical Cyclization. Synthesis of Cichorine (VI) and 4-Hydroxyisoindolin-1-one (VII) Natural Products.

✍ Scribed by German Lopez-Valdez; Simon Olguin-Uribe; Alejandra Millan-Ortiz; Rocio Gamez-Montano; Luis D. Miranda


Publisher
John Wiley and Sons
Year
2011
Weight
34 KB
Volume
42
Category
Article
ISSN
0931-7597

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✦ Synopsis


Abstract

An efficient access towards isoindolinones (V) is presented, involving the synthesis of thermally stable carbamoylxanthates (IV) from N‐tert‐butyl‐N‐benzylamines (I), the generation of the corresponding carbamoyl radicals and their cyclization—rearomatization reaction.