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ChemInform Abstract: Chemoselectivity and Mechanism of Desilylation of tert-Butyldimethylsilyl Ethers with TMSOTf.

โœ Scribed by Roger Hunter; Wolfgang Hinz; Philip Richards

Publisher
John Wiley and Sons
Year
2010
Weight
30 KB
Volume
30
Category
Article
ISSN
0931-7597

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ChemInform Abstract: Desilylation of t-B
ChemInform Abstract: Desilylation of t-Butyldimethylsilyl Ethers of Hydroxyquinones.
โœ Maria N. Bakola-Christianopoulou; Katerina K. Apazidou ๐Ÿ“‚ Article ๐Ÿ“… 2010 ๐Ÿ› John Wiley and Sons โš– 33 KB ๐Ÿ‘ 1 views

Desilylation of t-Butyldimethylsilyl Ethers of Hydroxyquinones. -The most general of three applied different desilylating procedures is the cleavage of the O-Si bond with Bu 4 NF. The other two methods use KF as desilylating agent in either the presence of a catalytic amount HBr, or basic Al 2 O 3 .