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ChemInform Abstract: Chemoenzymatic Synthesis of Enantiomerically Pure Alkene 1,2-Diols and Glycosides Thereof.

✍ Scribed by T. ZIEGLER; F. BIEN; C. JURISCH

Publisher: John Wiley and Sons
Year: 2010
Weight: 36 KB
Volume: 29
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199834052

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✦ Synopsis

Chemoenzymatic Synthesis of Enantiomerically Pure Alkene 1,2-Diols and Glycosides Thereof.

-In connection with a program aimed towards the chemoenzymatic synthesis of novel non-natural saccharides the kinetic resolution of alkene diols is investigated. Pseudomonas lipase catalyzed saponification and acetylation respectively are found to be suitable for large scale resolution of the title compounds (I) and (VIII). All enantiomerically pure alcohols are readily glycosylated with glycosyl halides and trichloroacetimidates.

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