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ChemInform Abstract: Cation Effects on the Voltammetric Behavior of α-Keggin-Type [SiMo12O40]4- and [PMo12O40]3- Complexes in CH3COCH3 and CH3CN.

✍ Scribed by Sadayuki Himeno; Masayo Takamoto; Tadaharu Ueda

Publisher
John Wiley and Sons
Year
2000
Weight
35 KB
Volume
31
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

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Bromohexyl)-3¢,4¢-ethylenedioxy)-2,2¢-bithiophene (3): Into a roundbottomed flask were introduced EDOT (5.9 g, 41.4 mmol) and 150 mL of tetrahydrofuran (THF). The mixture was cooled to ±40 C and butyllithium, 2.5 M in hexanes (19 mL, 47.5 mmol), was added rapidly. After 1 h stirring, tributyltin chl