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ChemInform Abstract: Callipeltoside A: Assignment of Absolute and Relative Configuration by Total Synthesis.

✍ Scribed by Barry M. Trost; Olivier Dirat; Janet L. Gunzner

Publisher: John Wiley and Sons
Year: 2010
Weight: 26 KB
Volume: 33
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200230251

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Callipeltoside A: Assignment of Absolute

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Callipeltoside A: Assignment of Absolute

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Total Synthesis and Absolute Configuration of Polycavernoside A. -The first total synthesis of polycavernoside A (XII), a toxin of red alga species, is presented, involving formation of the cyclic acetal (IV), lactonization of secoic acid (V) and rearrangement of the obtained 12-membered lactone (V