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ChemInform Abstract: Asymmetric Alkylation of β-Ketoesters.

✍ Scribed by B. M. TROST; R. RADINOV; E. M. GRENZER

Publisher
John Wiley and Sons
Year
2010
Weight
33 KB
Volume
28
Category
Article
ISSN
0931-7597

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✦ Synopsis

1997 stereochemistry stereochemistry (general, optical resolution) O 0030

49 -038

Asymmetric Alkylation of β-Ketoesters.

-The first examples of catalytic asymmetric alkylation of β-keto esters with high e.e.'s are reported. The method is applied to the synthesis of the alkaloid (-)-nitramine (X) in 6 steps and 43% overall yield. -(TROST,

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