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ChemInform Abstract: An Unusual Non-Radical Phenolic Coupling.

✍ Scribed by N. V. BELL; W. R. BOWMAN; P. F. COE; A. T. TURNER; D. WHYBROW

Publisher
John Wiley and Sons
Year
2010
Weight
29 KB
Volume
28
Category
Article
ISSN
0931-7597

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## Abstract The EPR spectrum of doxyl cyclododecane (3,3‐dimethyl‐1‐oxa‐4‐azaspiro[4.11] hexadec‐4‐yloxy) exhibits a large (0.195 mT at βˆ’39Β°C) temperature‐dependent proton hyperfine coupling. Selective deuteration demonstrates that the coupling is to one of the protons in the CH~2~ groups adjacent