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ChemInform Abstract: An Unconventional Method for Purifying the N-Carboxyanhydride Derivatives of γ-Alkyl-L-glutamates.

✍ Scribed by Drew S. Poche; Michael J. Moore; Jennifer L. Bowles

Publisher
John Wiley and Sons
Year
2010
Weight
31 KB
Volume
30
Category
Article
ISSN
0931-7597

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✦ Synopsis

An Unconventional Method for Purifying the N-Carboxyanhydride Derivatives of γ-Alkyl-L-glutamates. -Impurities found after synthesis of NCA derivatives of amino acids can be effectively removed by washing the reaction mixture with water and aqueous bicarbonate at 0 • C, despite the well known sensitivity of the NCA to water. -(POCHE, DREW S.; MOORE,

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