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ChemInform Abstract: An Improved Synthesis of the (E,Z)-Dienoate Precursor of (+)-Damavaricin D via a Vinylogous Horner—Wadsworth—Emmons Reaction.

✍ Scribed by Sherry R. Chemler; D. Scott Coffey; William R. Roush

Publisher: John Wiley and Sons
Year: 2010
Weight: 31 KB
Volume: 30
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199919259

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✦ Synopsis

An Improved Synthesis of the (E,Z)-Dienoate Precursor of (+)-Damavaricin D via a Vinylogous Horner-Wadsworth-Emmons Reaction.

-An improved synthesis of the title compound, the DmD intermediate (IV), is achieved by a (Z)-selective olefination of the aldehyde (III) using the vinylogous Horner-Wadsworth-Emmons reagent (II). -(CHEM-

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