A solution of bromine (8.0 g. 50 mmol) in pentane (50 mL) was added dropwise to a solution of [{Li,(NtBu),S),] (14.8 g, 25 mmol) in pentane (50 mL) at -78 'C. After the reaction mixture was stirred for 1 h a t room temperature, the solvent was removed in vacua, and the crude product condensed in a c
β¦ LIBER β¦
ChemInform Abstract: A Restitutive Bergman Rearrangement: Synthesis of a CpCo-Complexed Tetraethynylated Cyclobutadiene.
β Scribed by M. ALTMANN; G. ROIDL; V. ENKELMANN; U. H. F. BUNZ
- Book ID
- 101848687
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 28 KB
- Volume
- 28
- Category
- Article
- ISSN
- 0931-7597
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