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ChemInform Abstract: A Rearrangement of O,O-Silylketene Acetals Leading to γ-Thiomethylation of Butenoic Acid Derivatives.

✍ Scribed by L. JAROSKOVA; M. BOURGAUX; I. WENKIN; L. GHOSEZ

Publisher
John Wiley and Sons
Year
2010
Weight
33 KB
Volume
29
Category
Article
ISSN
0931-7597

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✦ Synopsis

Thiomethylation of Butenoic Acid Derivatives. -Ketene acetals (II) derived from the methylthiomethyl unsaturated esters (Ia) and (Ib) rearrange in refluxing toluene to give, after methanolysis, the γ-methylthiomethyl substituted methyl esters (IV), while in the case of phenylthiomethyl ester (Ic) the product (Vc) of α-substitution is also observed. -(JAROSKOVA, L.; BOURGAUX,

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