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ChemInform Abstract: A One-Pot Cross-Metathesis/Allylboration Reaction: A Three-Component Coupling for the Synthesis of Functionalized Homoallylic Alcohols.

✍ Scribed by Steven D. Goldberg; Robert H. Grubbs

Publisher: John Wiley and Sons
Year: 2010
Weight: 33 KB
Volume: 33
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200231068

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General procedure: A flame-dried round-bottomed flask was charged with 4 (1 equiv) and the olefin cross partner (3.0 equiv). A rubber septum was attached, dichloromethane was added (0.2 ± 0.3 n in 4), and argon was bubbled through the resultant solution for 10 min. Under a stream of argon, 3 (0.050

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