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ChemInform Abstract: A Novel Thiol-Protecting Group: A 2-Thioquinoline Sulfide as a Masked Sulfhydryl Moiety.

✍ Scribed by Jiancun Zhang; Mark D. Matteucci

Publisher
John Wiley and Sons
Year
2010
Weight
34 KB
Volume
30
Category
Article
ISSN
0931-7597

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✦ Synopsis

A 2-Thioquinoline Sulfide as a Masked Sulfhydryl Moiety.

-2-Thioquinoline (II) is easily introduced through S N 2 displacement with the thymidine analogue (I). It serves as masked sulfhydryl entity which is stable against bases, acids, and nucleophiles. Unmasking is readily achieved by NaBH 3 CN in acetic acid and following hydrolysis. -

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