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ChemInform Abstract: A Novel Route to the Fused Maleic Anhydride Moiety of CP Molecules.

✍ Scribed by K. C. Nicolaou; Phil S. Baran; Rolf Jautelat; Yun He; Kin Chiu Fong; Ha-Soon Choi; Won Hyung Yoon; Yong-Li Zhong

Publisher: John Wiley and Sons
Year: 2010
Weight: 24 KB
Volume: 30
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199923283

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A seven-step cascade reaction-in which selective mesylation, epoxide formation, epoxide lysis, cyclization, reiterative oxidation, and nitrogen-oxygen exchange occur sequentially-facilitates the construction of the maleic anhydride moiety of CP molecules 1 and 2 (>93% yield per step). Unstable inter

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