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ChemInform Abstract: A New Synthesis of α,β-Unsaturated N-Methoxy-N-methylamides.

✍ Scribed by C. BENEY; A. BOUMENDJEL; A.-M. MARIOTTE

Publisher: John Wiley and Sons
Year: 2010
Weight: 33 KB
Volume: 29
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199842076

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✦ Synopsis

1998 carboxylic amides carboxylic amides (acyclic compounds) P 0320

42 -076

A New Synthesis of α,β-Unsaturated N-Methoxy-N-methylamides.

-A new method to synthesize Weinreb-amides of type (III) by homologation of alkylhalides is reported. Sulfoxide (I) is synthesized in two steps with an overall yield of 45% from the corresponding chloroethanamide. -(BENEY,

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