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ChemInform Abstract: A General Solution Route Toward Metal Boride Nanocrystals.

✍ Scribed by David Portehault; Sarala Devi; Patricia Beaunier; Christel Gervais; Cristina Giordano; Clement Sanchez; Markus Antonietti

Book ID
102063422
Publisher
John Wiley and Sons
Year
2011
Weight
20 KB
Volume
42
Category
Article
ISSN
0931-7597

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✦ Synopsis

A General Solution Route Toward Metal Boride Nanocrystals. -Nanocrystals of NbB2, CaB6, HfB2, CeB6, MoB4, FeB, and Mn2B are prepared by reaction of the corresponding metal chlorides and sodium borohydride in a eutectic LiCl/KCl melt (Ar flow, 700-900 Β°C, 4 h). The samples are characterized by XRD, SEM, and TEM. This ionothermal process is applicable to a wide range of compounds and enables the formation of novel nanostructures and control over the nanocrystal size and the material texture. Processing of the nanoparticles within borosilicate glass-ceramic composites and tuning of the material conductivity are also described. -(PORTEHAULT*, D.; DEVI,

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