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ChemInform Abstract: 2,5-Bisdiazomethylfuran: A Novel Entry to the C6H4O Surface.

✍ Scribed by W. SANDER; R. ALBERS; P. KOMNICK; H. WANDEL

Publisher
John Wiley and Sons
Year
2010
Weight
27 KB
Volume
28
Category
Article
ISSN
0931-7597

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2,5-Bisdiazomethylfuran: A Novel Entry t
2,5-Bisdiazomethylfuran: A Novel Entry to the C6H4O Surface
✍ Sander, Wolfram ;Albers, Reinhard ;Komnick, Peter ;Wandel, Holger πŸ“‚ Article πŸ“… 1997 πŸ› John Wiley and Sons 🌐 English βš– 436 KB

## Abstract Warming the dilithium salt 7 of furan‐2,5‐dicarboxaldehyde bis(tosylhydrazone) to 110Β°C and subsequently trapping the products in solid argon at 10 K resulted in the formation of 1‐diazo‐hex‐3‐en‐5‐yn‐2‐one (9). The intermediate 2,5‐bis(diazomethylfuran) (6) is too labile to be directly