ChemInform Abstract: 2-Chloro-2-phenyl-2-(p-tolylthio)-1,3-diorgano-1,3,2λ5- diazaphosphetidin-4-ones.
✍ Scribed by V. A. PINCHUK; I. NEDA; C. MUELLER; A. FISCHER; P. G. JONES; YU. G. SHERMOLOVICH; R. SCHMUTZLER
- Book ID
- 112020601
- Publisher
- John Wiley and Sons
- Year
- 2010
- Weight
- 31 KB
- Volume
- 26
- Category
- Article
- ISSN
- 0931-7597
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The title compound, C 15 H 11 ClN 2 S, has been prepared by the reaction of Lawesson's reagent with N-(2-chlorobenzoyl)-N H -(4-methylbenzoyl)hydrazine, under microwave irradiation and in the absence of solvent. It crystallizes with two molecules per asymmetric unit and X-ray analysis reveals that t