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ChemInform Abstract: 1,8-Bis(phosphanyl)naphthalenes: 1,8-Bis((diethylamino)phosphanyl) naphthalene, 1,8-Bis(dichlorophosphanyl)naphthalene, and 1,3-Dichloro- 2,3-dihydro-1,3-dioxo-2-oxa-1,3-diphosphaphenalene.

✍ Scribed by A. KARACAR; H. THOENNESSEN; P. G. JONES; R. BARTSCH; R. SCHMUTZLER

Publisher: John Wiley and Sons
Year: 2010
Weight: 28 KB
Volume: 28
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199752182

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Structure and IR spectroscopic behaviour

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X-ray diffraction and IR spectroscopic studies on the proton sponge 2,7-dichloro-1,8-bis(dimethylamino)naphthalene and its adduct with HBr were performed. It was shown that the presence of the chlorine atoms in positions 2 and 7 leads to some change of conformation with respect to the free molecule.