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ChemInform Abstract: 1,5-Dimethyl-2,3,3,4-tetrachloro-1,5,2,4-diazadiphosphorinan-6-one and Some Derivatives. Part 2.

✍ Scribed by J. KRILL; I. V. SHEVCHENKO; A. FISCHER; P. G. JONES; R. SCHMUTZLER

Publisher: John Wiley and Sons
Year: 2010
Weight: 33 KB
Volume: 28
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.199731160

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Structure of thecis andtrans Isomers of

Structure of thecis andtrans Isomers of 2,4-Bis(diethylamino)-1,5-dimethyl-1,5,2,4-diazadiphosphorinan-6-one 2,4-Disulfide

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The 2,4-bis(dialkylamino)-1,5-dimethyl-1,5,2,4-diazadiphosphorinan-6-ones la and lb (R = CH3, a; C2H5, b) are thermally unstable. and are transformed into the bicyclic species 2 when heated to 150°C (2 Torr). The reactions of la and lb with elemental sulfur lead to the P,P'-disulfides 4a and 4b as a