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Chemical Synthesis of a Tetrasaccharide Fragment Related to the Exopolysaccharide of Arthrobacter sp. CE-17

✍ Scribed by Gregor Lemanski; Thomas Ziegler

Publisher: John Wiley and Sons
Year: 2000
Tongue: English
Weight: 319 KB
Volume: 2000
Category: Article
ISSN: 1434-193X
DOI: 10.1002/(sici)1099-0690(200001)2000:1<181::aid-ejoc181>3.0.co;2-7

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✦ Synopsis

The tetrasaccharide 5-aminopentyl glycoside β-D-Manp-O-benzylidene-1-thio-β-D-glucopyranoside (1) and ethyl 2,3,4-tri-O-benzyl-1-thio-α-D-mannopyranoside (5) in 5 (1Ǟ4)-β-D-Glcp-(1Ǟ4)-α-L-Rhap-(1Ǟ3)-β-D-Glcp-1-O-(CH 2 ) 5 NH 2 (22 ) r el at ed to th e e xo po ly sa cc ha ri de of steps. Building block 20 was obtained by coupling N-Zprotected 5-aminopentyl 2-O-benzyl-4,6-O-benzylidene-β-Arthrobacter sp. CE-17 was synthesized by coupling of the properly protected disaccharide blocks β

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