𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Chemical shift tensor determination using magnetically oriented microcrystal array (MOMA): 13C solid-state CP NMR without MAS

✍ Scribed by R. Kusumi; F. Kimura; G. Song; T. Kimura

Book ID
119300299
Publisher
Elsevier Science
Year
2012
Tongue
English
Weight
599 KB
Volume
223
Category
Article
ISSN
1090-7807

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

13C MAS NMR Spectra ofcis,cis-Mucononitr
13C MAS NMR Spectra ofcis,cis-Mucononitrile in Liquid-Crystalline Media and in the Solid State. Orientation of the Carbon Chemical-Shift Tensors
✍ K.V. Ramanathan; N. Suryaprakash; C.L. Khetrapal; Edwin D. Becker; Klaus Eichele 📂 Article 📅 1996 🏛 Elsevier Science 🌐 English ⚖ 128 KB

The spinning sidebands observed in the 13 C MAS NMR spectra (Fig. 1a), oriented in a nematic phase and in the solid state of cis,cis-mucononitrile oriented in liquid-crystalline media and of are presented. As a consequence of the carbon-13 chemicalthe neat sample in the solid state are studied. Ther

Determination of the Peptide Torsion Ang
Determination of the Peptide Torsion Angle φ by15N Chemical Shift and13Cα-1HαDipolar Tensor Correlation in Solid-State MAS NMR
✍ M. Hong; J.D. Gross; W. Hu; R.G. Griffin 📂 Article 📅 1998 🏛 Elsevier Science 🌐 English ⚖ 214 KB

We demonstrate a dipolar-chemical shift correlation technique for sign-sensitive determination of the torsion angle in solid peptides and proteins under magic-angle spinning. The indirect dimension of the experiment is obtained by separate but synchronous evolution of the magnetization under the 15