Chemical-shift-anisotropy powder patterns by the two-dimensional angle-flipping approach. Effects of crystallite packing

A Robust Technique for Two-Dimensional S

A Robust Technique for Two-Dimensional Separation of Undistorted Chemical-Shift Anisotropy Powder Patterns in Magic-Angle-Spinning NMR

✍ S-F. Liu; J-D. Mao; K. Schmidt-Rohr 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 257 KB

A robust magic-angle-spinning experiment for separating undistorted, quasi-static chemical-shift powder patterns is presented. It is derived from the technique of R. Tycko, G. Dabbagh, and P. Mirau (1989, J. Magn. Reson. 85, 265), but uses 360 • instead of 180 • pulses. In combination with a suitabl