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Chemical shift anisotropy in powdered solids studied by 2D FT NMR with flipping of the spinning axis

✍ Scribed by Ad Bax; Nikolaus M Szeverenyi; Gary E Maciel


Publisher
Elsevier Science
Year
1983
Weight
212 KB
Volume
55
Category
Article
ISSN
0022-2364

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A high-resolution 13C-nmr study of colla
✍ Hazime SaitΓ΄; Ryoko Tabeta; Akira Shoji; Takuo Ozaki; Isao Ando; Teruo Miyata πŸ“‚ Article πŸ“… 1984 πŸ› Wiley (John Wiley & Sons) 🌐 English βš– 987 KB

We have recorded high-resolution l3C-nmr spectra of collagen fibrils in the solid state by the cross-polarization-magic-angle-spinning (CP-MAS) method and analyzed the spectra with reference to those of collagenlike polypetides. We used two kinds of model polypeptides to obtain reference 13C chemica