Chemical (knight) shift distortions of quadrupole-split deuteron powder spectra in solids

A simple procedure for the determination

A simple procedure for the determination of the quadrupole interaction parameters and isotropic chemical shifts from magic angle spinning NMR spectra of half-integer spin nuclei in solids

✍ Günter Engelhardt; Hubert Koller 📂 Article 📅 1991 🏛 John Wiley and Sons 🌐 English ⚖ 410 KB

## Abstract A simple procedure is presented for the determination of the asymmetry parameter of the electric field gradient, the quadrupole coupling constant, the second‐order quadrupolar shift and the isotropic chemical shift of quadrupolar nuclei with half‐integer spin directly from the experimen