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Characterization of Various Magnesium Oxides by XRD and1H MAS NMR Spectroscopy

✍ Scribed by Marı́a Angeles Aramendı́a; José Antonio Benı́tez; Victoriano Borau; César Jiménez; José Marı́a Marinas; José Rafael Ruiz; Francisco Urbano

Publisher
Elsevier Science
Year
1999
Tongue
English
Weight
127 KB
Volume
144
Category
Article
ISSN
0022-4596

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✦ Synopsis

A magnesium oxide obtained by thermal decomposition of commercially available magnesium hydroxide was refluxed in water and acetone in order to improve its chemical and textural properties with the purpose of using it as a support for metals in heterogeneous catalysts. X-ray diffraction, CO 2 chemisorption, and 1 H magic-angle spinning nuclear magnetic resonance were used to identify crystal phases, the number of basic sites, and the nature of OH groups in the oxide, respectively.

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