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Characterization of Tetra-aryl Benzene Isomers by Using Preparative Gas Chromatography with Mass Spectrometry, Nuclear Magnetic Resonance Spectroscopy, and X-ray Crystallographic Methods

✍ Scribed by Rühle, Christian P. G.; Niere, Julie; Morrison, Paul D.; Jones, Roderick C.; Caradoc-Davies, Tom; Canty, Allan J.; Gardiner, Michael G.; Tolhurst, Vicki-Anne; Marriott, Philip J.

Book ID
127158889
Publisher
American Chemical Society
Year
2010
Tongue
English
Weight
869 KB
Volume
82
Category
Article
ISSN
0003-2700

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Preparative high performance liquid chromatography (HPLC) coupled to tandem mass spectrometry has been used successfully for the isolation of several drug metabolites from urine. Nuclear magnetic resonance (NMR) spectroscopy has been employed to determine the exact chemical structure of these metabo