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Characterization of cyclotrimethylenetrinitramine (RDX) by N,H isotope analyses with pyrolysis–atmospheric pressure ionization tandem mass spectrometry

✍ Scribed by A. Peter Snyder; Johannes H. Kremer; Shirley A. Liebman; Michael A. Schroeder; Robert A. Fifer

Publisher
John Wiley and Sons
Year
1989
Tongue
English
Weight
743 KB
Volume
24
Category
Article
ISSN
1076-5174

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The oxidative pyrolysis-atmospheric-pressure chemical ionization tandem mass spectrometry (Py-APCI MS/MS) of cyclotrimethylenetrinitramine (RDX) was investigated under various sample introduction conditions. Subambient (0.97 atm) as opposed to ambient (0.98 atm) pressure (1 atm = 101.325 kPa) facili

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## Abstract Analytical pyrolysis‐atmospberic pressure ionization (Py‐API) tandem mass Spectrometry was used in the structure elucidation of the oxidalive and non‐oxidative thermal decomposition products of cyclotetramethylenetetranitramine (HMX). The [^15^NO~2~]‐, [^15^N~8~]‐ and [^2^H~8~]‐HMX isot